محمود عبد العليم علي علي الرميلي   

أستاذ مساعد بقسم الكيمياء كلية العلوم جامعة سوهاج

حاصل علي الماجستير جامعة سوهاج 2009

الدكتورا تعاون بين جامعة سوهاج وجامعة مانشستر ميتروبولتان انجلترا  2012

ابحاث ما بعد الدكتوراة بجامعة غرناطة - اسبانيا 2012-2015

ابحاث ما بعد الدكتوراة بجامعة بورجوس اسبانيا 6 شهور 2017

Skills

• Multi-step organic synthesis; air sensitive compound handling; high vacuum techniques; kinetic methods; experience in routine organic chemistry laboratory methods; preparation of organic compounds and fine chemicals on a scale from 1 mg  to  1 kg. At the same time a higher experience in carbine and ylides chemistry.

• Have extensive recent experience of carrying out organic synthesis, ideally with control of absolute and relative stereochemistry; Be proficient and meticulous in the characterization of organic compounds;
• Have demonstrable competence/success in these areas.

• Able to plan and execute synthetic schemes successfully and safely (which includes completion of appropriate prior risk assessment) with minimal supervision;

•  Able to analyze and optimise reaction processes, have the experience and skills independently to select and execute appropriate purification techniques for isolating analytically pure compounds on a range of reaction scales;
• Able to carry out, interpret and properly record the results of modern spectroscopic techniques, particularly NMR spectroscopy;
• Have a general broad working knowledge of modern organic synthesis, including understanding of reaction mechanisms, the ability to convey this understanding, and awareness of current important trends and developments reported in the recent literature. Particular evidence will be sought of: (i) deeper understanding of the applicant’s previous fields of research; (ii) independent intellectual and practical contributions to previous research projects; (iii) ability to bring such attributes to bear on the present project.
• Work supportively in a laboratory environment with junior co-workers;
• Analytical methods:  spectroscopy (FTIR, MS, 1H, 13C, 31P 1D/2D NMR and Mass spectroscopy), chromatography (TLC, HPLC, GC).
• Computer skills: MS Windows, MS Office, ChemOffice, ISISDraw/ISISBase.
• Teaching experience: general organic chemistry laboratory, industrial organic chemistry and conservation chemistry 4 semesters.

• Member of the organizing committee for 11th International Chemistry Conference and exhibition in Africa (The role of chemistry in Development of Africa) (11ICCA), 20-23 November, 2010, Luxor, Egypt.

• المنشورات و المؤلفات

Synthesis and Antimicrobial Screening of Fused Heterocyclic Pyridines

2018-09-01 11:24:28 | الكلمات المفتاحية Pyridines,

In an attempt to find a new class of antimicrobial agents, a series of pyridoxazepine, pyridothiazepine, triazepine, naphthyridine, pyridopyrimidine, and other related products containing pyridine moiety were synthesized _via_ the reaction of 2‐amino‐6‐chloro‐3,5‐dicyanopyridine 1 with nucleophilic chemical reagents. These compounds were screened for cytotoxicity and their antimicrobial activity. Most of products showed inhibitory effect. إقراء المزيد

A robust Synthesis and Characterization for Superparamagnetic CoFe2O4 Nanoparticles as an Efficient and Reusable Catalyst for Synthesis of some Heterocyclic rings in aqueous media.

2018-09-01 11:26:25 | الكلمات المفتاحية Superparamagnetic CoFe2O4 Nanoparticles,

A robust synthesis for magnetic CoFe2O4 nanoparticles via a hydrothermal technique was investigated. The prepared magnetic nanoparticles were characterized using powder X-ray diffraction, scanning, transmission and high-resolution transmission electron microscopies, energy-dispersive X-ray and infrared spectroscopies, thermogravimetric analysis and vibrating sample magnetometry. Based on the obtained data, the prepared powder was composed of ultrafine particles in nanometer size range with highly ... إقراء المزيد

Divinyl Sulfone Cross-Linked b-Cyclodextrin Polymer as New and Effective Corrosion Inhibitor for Zn Anode in 3.5 M KOH.

2018-09-01 11:29:32 | الكلمات المفتاحية Divinyl Sulfone Cross-Linked b-Cyclodext,

he inhibition behavior of the divinyl sulfone cross-linked β-cyclodextrin polymer (βCDS-P) in 3.5 M KOH in the temperature range 25–55 °C on Zn anode was studied using weight loss, potentiodynamic polarization and electrochemical impedance spectroscopy measurements. Results showed that, the inhibition efficiency increased with the increase in the concentration of inhibitor and the best inhibitor efficiency was reached with 250 ... إقراء المزيد

Synthesis and in vitro antibacterial evaluation of some novel fused pyridopyrimidine derivatives

2018-09-01 11:30:52 | الكلمات المفتاحية fused pyridopyrimidine derivatives,

Pyridopyrimidine derivatives 2, 5 and 7, 8, 9 were furnished by the reaction of compound 1 with a variety of reagents, namely, formic acid, acetic anhydride, phenyl isothiocyanate, phenyl isocyanate, carbon disulfide, acetamide and thioacetamide, which in turn were treated with hydrazine to give pyrazolopyridopyrimidine derivatives 4, 6 and 11, 12, 13. The potency of the results as antibacterial agents ... إقراء المزيد

Epichlorohydrin cross-linked β-cyclodextrin polymer a promising method in industry for the synthesis of 2-phenylbenzthiazole in water

2018-09-01 11:32:09 | الكلمات المفتاحية 2-phenylbenzthiazole in water,

In the present study, we report an environmentally benign synthesis of 2-arylbenzothiazoles derivatives from _o_-aminothiophenol and aldehydes in aqueous medium using _β_-cyclodextrin polymer as a catalyst and air as an oxidant. The polymer showed excellent catalytic activity, recovered, reused six times, and the catalyst efficiency remained unchanged. This suggests that the catalyst is an efficient and green catalyst for the ... إقراء المزيد

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