safa_elmasry

Safa El-masry

Teadching-Assistant - Lecturer

Faculty of science

Address: Sohag university-Faculty of science- Zoology department

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Publications Which contain the keyword: efficient catalyst


Green synthesis of TiO2 nanoparticles as an efficient heterogeneous catalyst with high reusability for synthesis of 1,2-dihydroquinoline derivatives
Nano materials find wide applications due to their behavior at nano scale. TiO2 nanoparticles (TiO2 NPs) was synthesized using Neem leaf extract. This is simple, rapid, eco-friendly, cheaper and green tools for TiO2 NPs synthesis using agricultural waste at lower applied temperature. Characterization of the extracted TiO2 NPs was confirmed by XRD, SEM, EDAX, TEM, HR-TEM, SAED, and FT-IR, respectively. ... Read more

Morpholinium hydrogen sulfate (MHS) ionic liquid  as an efficient catalyst for the synthesis of bio-active multi-substituted imidazoles (MSI) under  solvent-free conditions
Morpholinium hydrogen sulfate as an ionic liquid was employed as a catalyst for the synthesis of a biologically active series of multi-substituted imidazoles by a four-component reaction involving the combination of benzil with different aromatic aldehydes, ammonium acetate, and 1-amino-2-propanol under solvent-free con-ditions. The key advantages of this method are shorter reaction times, very high yield, and ease of processing. ... Read more

Hydrothermal preparation and characterization of ZnFe2O4 magnetic nanoparticles as an efficient heterogeneous catalyst for the synthesis of multi‐substituted imidazoles and study of their anti‐inflammatory activity
Nanoparticles are key focus of research for a wide range of novel applications. As such, ZnFe2O4 magnetic nanoparticles were synthesized hydrothermally and charac-terized via scanning and transmission electron microscopies, powder X‐ray diffrac-tion, energy‐dispersive X‐ray and infrared spectroscopies, thermogravimetric analysis and magnetic measurements. They were used as a robust catalyst for the synthesis of a series of biologically active multi‐substituted imidazoles ... Read more

Hydrothermal preparation and characterization of ZnFe2O4 magnetic nanoparticles as  catalyst for the synthesis of multi‐substituted imidazoles
Nanoparticles are key focus of research for a wide range of novel applications. As such, ZnFe2O4 magnetic nanoparticles were synthesized hydrothermally and characterized via scanning and transmission electron microscopies, powder X‐ray diffraction, energy‐dispersive X‐ray and infrared spectroscopies, thermogravimetric analysis and magnetic measurements. They were used as a robust catalyst for the synthesis of a series of biologically active multi‐substituted imidazoles ... Read more

Magnetic NiFe2O4 nanoparticles: efficient, heterogeneous and reusable catalyst for synthesis of acetylferrocene chalcones and their anti‐tumour activity
A robust synthesis of magnetic NiFe2O4 nanoparticles via a hydrothermal technique was investigated. The prepared magnetic NiFe2O4 nanoparticles were characterized using powder X‐ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), high‐resolution TEM, energy‐dispersive X‐ray spectroscopy, thermogravimetric analysis, infrared spectroscopy and vibrating sample magnetometry. XRD and TEM analyses confirmed the formation of single‐phase ultrafine nickel ferrite nanoparticles with highly ... Read more

CuFe2O4 nanoparticles: an efficient heterogeneous magnetically separable catalyst for synthesis of some novel propynyl-1H-imidazoles derivatives
The non-toxic magnetic CuFe2O4 nanoparticles have been synthesized, characterized, and used as an efficient catalyst for synthesis of new derivatives for 1,2,4,5-tetrasubstituted imidazoles in excellent yields. The synthesized compounds work-up easy and purification of products are performed without chromatographic methods. The catalyst can be recovered for the subsequent reactions and reused without any appreciable loss. Read more

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