omerelsheikh

omerelsheikh

مدرس - عضو هيئة تدريس

كلية العلوم

العنوان: Sohag

2

إعجاب

المنشورات و المؤلفات التي تحتوي علي الكلمة المفتاحية: In situ


A flexible gas flow reaction cell for in situ x-ray absorption spectroscopy studies
A capillary-based sample environment with hot air blower and integrated gas system was developed at Diamond to conduct X-ray absorption spectroscopy (XAS) studies of materials under time-resolved, _in situ_ conditions. The use of a hot air blower, operating in the temperature range of 298-1173 K, allows introduction of other techniques e.g. X-ray diffraction (XRD), Raman spectroscopy for combined techniques studies. ... إقراء المزيد

2018-11-01 02:56:32 الكلمات المفتاحية In situ, Advanced spectroscopy, EXAFS, MoOx/Fe2O3, DRIFTS, Methanol oxidation,
In situ spectroscopic investigations of MoOx/Fe2O3 catalysts for the selective oxidation of methanol
Multicomponent oxide shell@core catalysts have been prepared, affording overlayers of MoO_x_ on Fe2O3. This design approach allows bulk characterization techniques, such as X-ray Absorption Fine Structure (XAFS), to provide surface sensitive information. Coupling this approach with _in situ_ methodologies provides insights during crucial catalytic processes. Calcination studies were followed by a combination of XAFS and Raman, and demonstrate that amorphous ... إقراء المزيد

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