Three archaeological textiles fragments from three excavations in Sohag (The red Monastery, Abidus and Akhmeem) were investigated by means of Stereo Microscopy and Scanning Electron Microscopy (SEM), UV-Vis Spectrophotometer and X-ray fluorescence (XRF), as well as (FTIR). Many information have been obtained relating identification and characterization of dyestuffs, kind of the natural fibers and the determination of the kind of weave structure techniques used. Wool fibers were recognized in the recovered fragments. Plain weave with its derived weaves such as reps whether regular or irregular warp reps was identified. Fragments of textiles have also been found in various states of degradation.