A robust synthesis of magnetic NiFe2O4 nanoparticles via a hydrothermal technique was investigated. The prepared magnetic NiFe2O4 nanoparticles were characterized using powder X‐ray diffraction (XRD), scanning electron microscopy, transmission electron microscopy (TEM), high‐resolution TEM, energy‐dispersive X‐ray spectroscopy, thermogravimetric analysis, infrared spectroscopy and vibrating sample magnetometry. XRD and TEM analyses confirmed the formation of single‐phase ultrafine nickel ferrite nanoparticles with highly ...
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